ISSN: 2249-9504
CAS CODEN: IJPCDX

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Citations : 3566

International Journal of Pharmaceutical, Chemical and Biological Sciences received 3566 citations as per google scholar report

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STEPWISE SYNTHESIS AND CHARACTERIZATION OF NEWLY SYNTHESIZED 1,2,4-TRIAZOLE DERIVATIVES

Abstract

Author(s): Kavitha Siddoju1* and Jagadeesh Kumar Ega2

In this paper we would like to discuss the efficient synthesis of pyrazin fused N-(3-Mercapto-5-Aryl- [1,2,4]triazol-4-yl)-amide (5a-m and 6a-r) from4-Amino-5-Aryl-4H-[1,2,4]triazole-3-thiols(4a-b) through N-acylaton under dry dioxane, R1COCl, reflux, 10 h by a sequential manner probably the steps are mentioned in Scheme-1 ,Table-1,2. The structures of the compounds were elucidated by spectral (IR,1HNMR, 13CNMR and MS) analysis. The reactions are easy to conduct, under mild conditions, and form amide substituted triazole derivatives with excellent yields.

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